HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 86742492, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-(2-chloroethoxy)-2-nitrobenzene | HCID 4362487 | — |
| Reactant | HCID 21287188 | HCID 21287188 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86742492 | HCID 86742492 | 55.4% |
Reaction Steps
A mixture of 2-Nitrophenoxyethylchloride (0.26 g), 5-(3-Amino-propionyl)-1,5-benzothiazepine (0.355 g) and potassium carbonate (0.210 g) in toluene (15 ml) was refluxed for 16 hours. After cooling, objective compound (0.184 g) was obtained according to the method of experimental 1. m.p. 178°-180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780462 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-45b8551da0944f52ba6ba44b007c0cc5 |
| Source note | uspto-grants-1988_10 |