HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromoisatin → 5-Bromo-1-(2-diisopropylaminoethyl)isatin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromoisatin | HCID 6889 | — |
| Reactant | 2-Chloroethyldiisopropylammonium chloride | HCID 77942 | — |
| Product | 5-Bromo-1-(2-diisopropylaminoethyl)isatin | HCID 13934415 | 82.9% |
Reaction Steps
By using 5-bromoisatin and 2-diisopropylaminoethyl chloride hydrochloride, a method analogous to that described in Reference Example 7 was carried out to obtain 5-bromo-1-(2-diisopropylaminoethyl)isatin having a melting point of 91°-93° C. (yield: 82.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780477 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-2064c85ec7fc417fb4cd615a476618f6 |
| Source note | uspto-grants-1988_10 |