HuagongsheHuagongshe Chemistry Print Report · For research reference only
Semicarbazide hydrochloride → HCID 178457221, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Semicarbazide hydrochloride | HCID 11236 | — |
| Reactant | HCID 13934421 | HCID 13934421 | — |
| Product | HCID 178457221 | HCID 178457221 | 65.3% |
Reaction Steps
By using 1-(2-diisopropylamino-1-methylethyl)isatin and semicarbazide hydrochloride, a method analogous to that described in Example 10 was carried out and the reaction product was recrystallized from ethanol to obtain (E)-1-(2-diisopropylamino-1-methylethyl)isatin 3-semicarbazone having a melting point of 195°-197° C. (yield: 65.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780477 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-b160d800078c407a9cbd12b8d2d6877e |
| Source note | uspto-grants-1988_10 |