HRID868590

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11236

Semicarbazide hydrochloride

CH6ClN3O

结构：Cc1ccc2c(c1)C(=O)C(=O)N2CCN(C(C)C)C(C)C

HCID13934409

未命名化合物

PRODUCTS

生成物

$结构：Cc1ccc2c(c1)/C(=N\NC(N)=O)C(=O)N2CCN(C(C)C)C(C)C$

HCID178422541

未命名化合物

收率 53.9%

PROCEDURE

实验过程

By using 1-(2-diisopropylaminoethyl)-5-methylisatin and semicarbazide hydrochloride, a method analogous to that described in Example 4 was carried out to obtain (E)-1-(2-diisopropylaminoethyl)-5-methylisatin 3-semicarbazone having a melting point of 159°-161° C. (yield: 53.9%, recrystallizing solvent: chloroform-hexane).