HuagongsheHuagongshe Chemistry Print Report · For research reference only
Semicarbazide hydrochloride → HCID 178422541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Semicarbazide hydrochloride | HCID 11236 | — |
| Reactant | HCID 13934409 | HCID 13934409 | — |
| Product | HCID 178422541 | HCID 178422541 | 53.9% |
Reaction Steps
By using 1-(2-diisopropylaminoethyl)-5-methylisatin and semicarbazide hydrochloride, a method analogous to that described in Example 4 was carried out to obtain (E)-1-(2-diisopropylaminoethyl)-5-methylisatin 3-semicarbazone having a melting point of 159°-161° C. (yield: 53.9%, recrystallizing solvent: chloroform-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780477 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-4a6c65540ad14d73aff735467df2bc5e |
| Source note | uspto-grants-1988_10 |