HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Benzylsemicarbazide hydrochloride → HCID 178422543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Benzylsemicarbazide hydrochloride | HCID 12401712 | — |
| Reactant | HCID 13934409 | HCID 13934409 | — |
| Product | HCID 178422543 | HCID 178422543 | 74.6% |
Reaction Steps
By using 1-(2-diisopropylaminoethyl)-5-methylisatin and 4-benzylsemicarbazide hydrochloride, a method analogous to that described in Example 6 was carried out to obtain (E)-1-(2-diisopropylaminoethyl)5-methylisatin 3-(4-benzylsemicarbazone) having a melting point of 159°-160° C. (yield: 74.6%, recrystallizing solvent: ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780477 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-be2b3e13291749fd80e07041e1736677 |
| Source note | uspto-grants-1988_10 |