HuagongsheHuagongshe Chemistry Print Report · For research reference only
Semicarbazide hydrochloride → HCID 178457387, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Semicarbazide hydrochloride | HCID 11236 | — |
| Reactant | HCID 13934411 | HCID 13934411 | — |
| Product | HCID 178457387 | HCID 178457387 | 86.5% |
Reaction Steps
By using 1-(2-diisopropylaminoethyl)-5-fluoroisatin and semicarbazide hydrochloride, a method analogous to that described in Example 6 was carried out to obtain (E)-1-(2-diisopropylaminoethyl)-5-fluoroisatin 3-semicarbazone having a melting point of 158°-160° C. (yield: 86.5%, recrystallizing solvent: chloroform-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780477 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-1788772ef4384d5d9a4c0bf3445396f0 |
| Source note | uspto-grants-1988_10 |