HuagongsheHuagongshe Chemistry Print Report · For research reference only
Semicarbazide hydrochloride → HCID 178457385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Semicarbazide hydrochloride | HCID 11236 | — |
| Reactant | HCID 13934412 | HCID 13934412 | — |
| Product | HCID 178457385 | HCID 178457385 | 49.4% |
Reaction Steps
By using 5-chloro-1-(2-diisopropylaminoethyl)isatin and semicarbazide hydrochloride, a method analogous to that described in Example 4 was carried out to obtain (E)-5-chloro-1-(2-diisopropylaminoethyl)isatin 3-semicarbazone having a melting point of 154°-155° C. (yield: 49.4%, recrystallizing solvent: chloroform-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780477 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-549189e8914649f188239124b89a3030 |
| Source note | uspto-grants-1988_10 |