HuagongsheHuagongshe Chemistry Print Report · For research reference only
Semicarbazide hydrochloride → HCID 178449090, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Semicarbazide hydrochloride | HCID 11236 | — |
| Reactant | HCID 13934424 | HCID 13934424 | — |
| Product | HCID 178449090 | HCID 178449090 | 40.3% |
Reaction Steps
By using 1-(2-tert-butylaminoethyl)isatin and semicarbazide hydrochloride, a method analogous to that described in Example 10 was carried out, and the reaction product was recrystallized from ethanol to obtain (E)-1-(2-tert-butylaminoethyl)isatin 3-semicarbazone having a melting point of 173°-176° C. (decomposition) (yield: 40.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780477 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-7f8a52b057344d39bc796f90cad73cee |
| Source note | uspto-grants-1988_10 |