HuagongsheHuagongshe Chemistry Print Report · For research reference only
Semicarbazide hydrochloride → HCID 178457377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Semicarbazide hydrochloride | HCID 11236 | — |
| Reactant | 1-[2-(N-isopropylbenzylamino)ethyl]isatin | HCID 54367399 | — |
| Product | HCID 178457377 | HCID 178457377 | 52.7% |
Reaction Steps
By using 1-[2-(N-isopropylbenzylamino)ethyl]isatin and semicarbazide hydrochloride, a method analogous to that described in Example 6 was carried out to obtain (E)-1-[2-(N-isopropylbenzylamino)ethyl]isatin 3-semicarbazone having a melting point of 193°-194° C. (yield: 52.7%, recrystallizing solvent: ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780477 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-2604685e364a4854811e5a276a6ebe1b |
| Source note | uspto-grants-1988_10 |