Ethanol → 71937-06-9

HRID 868608Notes

Reaction equation

HRID 868608 reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=1.[Cl:11][C:12]1[CH:19]=[C:16]([CH:17]=O)[C:15]([OH:20])=[CH:14][CH:13]=1.C(O)C>CO>[Cl:11][C:12]1[CH:13]=[CH:14][C:15]([OH:20])=[C:16]([CH:19]=1)[CH:17]=[N:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=1

Participants

5

Reactant 3

HCID 702EthanolHCID 9784-Aminobenzoic AcidHCID 124815-Chloro-salicylaldehyde

Product 1

HCID 96143171937-06-9Yield 94%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using the procedure of Sheeman et al [J.A.C.S., Vol. 84 (1982), p. 2457], 1.37 g of p-amino-benzoic acid, 2.35 g of 5-chlorosalicylaldehyde, 240 ml of ethanol and 17 ml of anhydrous methanol were reacted to obtain 2.59 g of 4-[(5-chloro-2-hydroxy-benzylidene)amino]-benzoic acid.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-aa5912f4ae8f4d76baf44bacfdb70c76
Source dataset
uspto-grants-1988_10
Patent number
US04780504

Reaction notes

Loading…