HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 71937-06-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Aminobenzoic Acid | HCID 978 | — |
| Reactant | 5-Chloro-salicylaldehyde | HCID 12481 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 71937-06-9 | HCID 961431 | 94% |
Reaction Steps
Using the procedure of Sheeman et al [J.A.C.S., Vol. 84 (1982), p. 2457], 1.37 g of p-amino-benzoic acid, 2.35 g of 5-chlorosalicylaldehyde, 240 ml of ethanol and 17 ml of anhydrous methanol were reacted to obtain 2.59 g of 4-[(5-chloro-2-hydroxy-benzylidene)amino]-benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780504 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-aa5912f4ae8f4d76baf44bacfdb70c76 |
| Source note | uspto-grants-1988_10 |