HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 135617149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 5-Chloro-salicylaldehyde | HCID 12481 | — |
| Reactant | (3-Aminophenyl)acetic acid | HCID 571807 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 135617149 | HCID 135617149 | 69.6% |
Reaction Steps
Using the procedure of Sheeman et al [J.A.C.S., Vol. 84, (1982), p. 2457], 1.5 g of 3-amino-phenylacetic acid, 1.72 g of 5-chloro-2-hydroxy-benzaldehyde, 480 ml of 100% ethanol and 35 ml of methanol were reacted to obtain 2 g of 3-[(5-chloro-2-hydroxy-benzylidene)-amino]-phenylacetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780504 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-e3f23a4fdd774b15b8fdf7211d3fc8d4 |
| Source note | uspto-grants-1988_10 |