HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methylbenzofuran → HCID 14257620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methylbenzofuran | HCID 86929 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14257620 | HCID 14257620 | — |
Reaction Steps
6-Methylbenzofuran (15 g) was dissolved in methanol (200 ml) containing 0.5 g of 10% palladium on carbon. This solution was shaken on a Paar hydrogenator under hydrogen at 40 psi. When hydrogen uptake was complete, the solution was filtered through Celite and the ethanol evaporated to yield 6-methyl-2,3-dihydrobenzofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780480 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-1957b114f40e408c93883833b0b7ccc0 |
| Source note | uspto-grants-1988_10 |