Aniline → Aniline

HRID 868632Notes

Reaction equation

HRID 868632 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S:8]1[C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=2[N:10]=[CH:9]1.[S].C(=S)=[S:19]>>[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[SH:19][C:9]1[S:8][C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=2[N:10]=1

Participants

6

Reactant 4

HCID 6115AnilineHCID 6348Carbon DisulfideHCID 7222BenzothiazoleHCID 5362487Sulfur

Product 2

HCID 6115AnilineHCID 178418395HCID 178418395, compound

Procedure

The distillates containing aniline and benzothiazole, can be reacted with carbon disulphide and sulphur, if appropriate together with fresh aniline and/or benzothizole, in a known manner to give highly pure 2-mercaptobenzothiazole.

Sources & evidence

ORD record
ord-2f3bdb7269474077902c6930c4337482
Source dataset
uspto-grants-1988_10
Patent number
US04780540

Reaction notes

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