HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 21287654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | HCID 67938254 | HCID 67938254 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 21287654 | HCID 21287654 | — |
Reaction Steps
A solution of 4.1 grams (20 millimoles) of methyl 3-(2-methylphenyl)aminocrotonate in 5 milliliters of dry benzene is added to the titanamine complex followed by 1.1 grams (10 millimoles) of benzaldehyde and the mixture stirred at ambient temperature for several hours to obtain the desired dimethyl 2,6-dimethyl-4-phenyl-1-(2-methylphenyl)-1,4-dihydropyridine-3,5-dicarboxylate which may be recovered in a manner similar to that previously described.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780538 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-1859e008b4b74498bc5f38b89dcabfd6 |
| Source note | uspto-grants-1988_10 |