HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethyl methyl sulfide → (n-Hexylthio) Ethyl Isothiocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethyl methyl sulfide | HCID 10965 | — |
| Reactant | 1-((2-Chloroethyl)thio)hexane | HCID 12260279 | — |
| Reactant | n-C6H13SCH2CH2SCN | HCID 131715735 | — |
| Product | (n-Hexylthio) Ethyl Isothiocyanate | HCID 53861891 | — |
Reaction Steps
Example 1 is repeated with the exception that n-C6H13SCH2CH2Cl is used as a reagent instead of CH3SCH2CH2Cl and the reaction is allowed to proceed for seventy-five minutes. The product is isolated by distillation at reduced pressure and analyzed by gas chromatography/mass spectrometry which shows that the product is 0.7 percent n-C6H13SCH2CH2SCN and 97.0 percent n-C6H13SCH2CH2NCS.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780557 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-8ef64004375d4d72b748aa63791b4535 |
| Source note | uspto-grants-1988_10 |