HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H,3H-Thieno[3,4-c]furan-1,3-dione → HCID 67054651, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H,3H-Thieno[3,4-c]furan-1,3-dione | HCID 315608 | — |
| Reactant | HCID 66794687 | HCID 66794687 | — |
| Solvent | Acetic acid ethanol | HCID 18476134 | — |
| Product | HCID 67054651 | HCID 67054651 | — |
Reaction Steps
A mixture of 4,5-bis((2-ethylhexyl)oxy)benzene-1,2-diamine (5.8 g, 0.016 mol) and thieno[3,4-c]furan-1,3-dione (2.5 g, 0.016 mol) is refluxed in a 100 mL acetic acid:ethanol (1:1) solvent blend for 24 hours. The solvent is distilled off and the crude product is purified by column chromatography (CHCl3) to yield the final product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08968885B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-714a835fbe284f4f9b26dd3ebbd92805 |
| Source note | uspto-grants-2015_03 |