HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86729187, compound → HCID 71295260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86729187 | HCID 86729187 | — |
| Reactant | HCID 86729188 | HCID 86729188 | — |
| Product | HCID 71295260 | HCID 71295260 | 16% |
Reaction Steps
85 mg of tert-butyl 4-(6-aminopyridin-3-yl)pyrazole-1-carboxylate are reacted with 100 mg of 5-(2-chloropyridin-4-yl)-2-(tetrahydropyran-4-yloxy)benzonitrile in accordance with the above-mentioned general procedure for the Buchwald-Hartwig reaction, giving the desired product in 16% yield;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969335B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-22ae0a203cc74eaa9a0ca212e018f31e |
| Source note | uspto-grants-2015_03 |