1-(2-Chloroethyl)pyrrolidine hydrochloride → HCID 86723173, compound

Participants

Reaction Steps

The title compound was prepared from 5-chloro-3-iodo-indazole and 1-(2-chloroethyl)pyrrolidine hydrochloride in 60% yield according to the procedure for Preparation 50A. 1H NMR (400 MHz, CDCl3): δ 1.75-1.80 (4H, m), 2.54-2.59 (4H, m), 2.99 (2H, t, J=7.3 Hz), 4.52 (2H, t, J=7.1 Hz), 7.35-7.39 (2H, m), 7.45 (1H, s). [M+H] Calc'd for C13H15ClN3, 376; Found, 376.

Provenance & Evidence