HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70648558, compound → HCID 70098706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70648558 | HCID 70648558 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 70098706 | HCID 70098706 | 69.5% |
Reaction Steps
A solution of 2-(3-(1-(N,N-dimethylsulfamoyl)-4-phenyl-1H-imidazol-2-yl)propanamido)benzoic acid (150 mg, 0.339 mmol) in Ac2O (10 mL) was stirred at reflux for 5 h. The reaction mixture was then concentrated to give a white solid (100 mg), which was used for the next step without further purification. LC-MS: m/z 425 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969349B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-948a8bcbccd14c54bf51cddbb291fd31 |
| Source note | uspto-grants-2015_03 |