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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 868913Generated: October 28, 2026

HCID 70648558, compound → HCID 70098706, compound

https://huagongshe.com/reaction/868913

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 70648558HCID 70648558—
SolventAcetic AnhydrideHCID 7918—
ProductHCID 70098706HCID 7009870669.5%

Reaction Steps

A solution of 2-(3-(1-(N,N-dimethylsulfamoyl)-4-phenyl-1H-imidazol-2-yl)propanamido)benzoic acid (150 mg, 0.339 mmol) in Ac2O (10 mL) was stirred at reflux for 5 h. The reaction mixture was then concentrated to give a white solid (100 mg), which was used for the next step without further purification. LC-MS: m/z 425 (M+H+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08969349B2
Source datasetuspto-grants-2015_03
ORD IDord-948a8bcbccd14c54bf51cddbb291fd31
Source noteuspto-grants-2015_03