Thionyl Chloride → HCID 70098970, compound

HRID 868938Notes

Reaction equation

HRID 868938 reaction equation
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=[CH:3][C:2]=1[CH:11](O)[CH2:12][C:13]1[CH:22]=[N:21][C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[N:14]=1.O=S(Cl)[Cl:26]>>[Cl:26][CH:11]([C:2]1[CH:3]=[N:4][C:5]2[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=2)[N:1]=1)[CH2:12][C:13]1[CH:22]=[N:21][C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[N:14]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 70648559HCID 70648559, compound

Product 1

HCID 70098970HCID 70098970, compound

Procedure

A solution of 1,2-di(quinoxalin-2-yl)ethanol (0.05 g, 0.166 mmol) in SOCl2 (2 mL) was stirred at room temperature for 1 hour. The solution was then concentrated to afford 2,2′-(1-chloroethane-1,2-diyl)diquinoxaline (0.05 g) as a yellow solid. MS (ESI) m/z 321.1 (M+H+).

Workup

  1. concentrationThe solution was then concentrated

Sources & evidence

ORD record
ord-cafb8b70d0ee4b13beba8a833270e11f
Source dataset
uspto-grants-2015_03
Patent number
US08969349B2

Reaction notes

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