HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 70098970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 70648559 | HCID 70648559 | — |
| Product | HCID 70098970 | HCID 70098970 | — |
Reaction Steps
A solution of 1,2-di(quinoxalin-2-yl)ethanol (0.05 g, 0.166 mmol) in SOCl2 (2 mL) was stirred at room temperature for 1 hour. The solution was then concentrated to afford 2,2′-(1-chloroethane-1,2-diyl)diquinoxaline (0.05 g) as a yellow solid. MS (ESI) m/z 321.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969349B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-cafb8b70d0ee4b13beba8a833270e11f |
| Source note | uspto-grants-2015_03 |