反应详情

A solution of tert-butyl mesitylsulfonyloxycarbamate (3 g, 9.5 mmol) in trifluoroacetic acid (7 mL) was stirred at 10° C. for 40 min, then poured into ice/water (10 mL) and the resulting solid was collected by filtration. The solid was dissolved in DCM (12 mL), dried with Na2SO4, and filtered. The solution containing O-(mesitylsulfonyl)hydroxylamine was used without further purification.

1. filtrationthe resulting solid was collected by filtration
2. dissolutionThe solid was dissolved in DCM (12 mL)
3. dry with materialdried with Na2SO4
4. filtrationfiltered
5. additionThe solution containing O-(mesitylsulfonyl)hydroxylamine
6. customwas used without further purification