化工社化工社 化学情報印刷レポート · 研究参考用
7-Methoxyquinoline-8-carboxylic acid → 7-Hydroxyquinoline-8-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 7-Methoxyquinoline-8-carboxylic acid | HCID 68774583 | — |
| 溶媒 | Hydrogen Bromide | HCID 260 | — |
| 生成物 | 7-Hydroxyquinoline-8-carboxylic acid | HCID 135881555 | — |
反応手順
The title compound of Step A (2.9 g, 14.1 mmol) in HBr (14 mL) was heated at 90° C. for 1 h. The mixture was then concentrated washed with PhCH3 and used without further purification in subsequent steps.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08969352B2 |
| 出典データセット | uspto-grants-2015_03 |
| ORD ID | ord-fd5a47708d0f43f8bb73ea41a9c0c9c6 |
| 出典メモ | uspto-grants-2015_03 |