Acetyl chloride → HCID 53497003, compound

Participants

Reaction Steps

To a solution of 5-(6-(2-(4-fluorophenyl)-2-methylpropylamino)pyridazin-3-yl)-1H-indazol-3-amine (50 mg, 133 μmol) in pyridine (1 mL) was added acetyl chloride (9.5 μL, 133 μmol). The mixture was stirred for 15 min, concentrated, purified by reverse phase chromatography using a CH3CN/water gradient to afford 25 mg of white solid, m/z=419.9 [M+H].

Provenance & Evidence