HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → 9-(2-Bromoethyl)-2-butoxy-8-methoxy-9H-purin-6-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178450370 | HCID 178450370 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 9-(2-Bromoethyl)-2-butoxy-8-methoxy-9H-purin-6-amine | HCID 58942893 | — |
Reaction Steps
The compound obtained in Example 2-1 step (v) (2 g), potassium carbonate (3.7 g) and 1,2-dibromoethane (0.6 ml) were added to dimethylformamide (20 ml), and the same manner to Example 2-13 step (i) was conducted to give the titled compound as a cream colored solid. Yield: 1.2 g (62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969362B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-592d3cb600b048e3b2c956eb6392f8cd |
| Source note | uspto-grants-2015_03 |