1,3-Dibromopropane → HCID 58552035, compound

HRID 869362Notes

Reaction equation

HRID 869362 reaction equation
[Br:1][CH2:2][CH2:3][CH2:4]Br.[NH2:6][C:7]1[CH:8]=[C:9]([CH2:13][C:14]([O:16][CH3:17])=[O:15])[CH:10]=[CH:11][CH:12]=1>>[Br:1][CH2:2][CH2:3][CH2:4][NH:6][C:7]1[CH:8]=[C:9]([CH2:13][C:14]([O:16][CH3:17])=[O:15])[CH:10]=[CH:11][CH:12]=1

Participants

3

Reactant 2

HCID 80011,3-DibromopropaneHCID 13054266Methyl 3-aminophenylacetate

Product 1

HCID 58552035HCID 58552035, compound

Procedure

Using 1,3-dibromopropane (1.7 ml) and methyl (3-aminophenyl)acetate (280 mg), the same manner to Example 2-41 step (i) was conducted to give the titled compound as a solid. Yield: 200 mg (70%).

Sources & evidence

ORD record
ord-a11190ab510b48ff958363a06ef3d48f
Source dataset
uspto-grants-2015_03
Patent number
US08969362B2

Reaction notes

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