Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 86722254 | HCID 86722254 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178488260 | HCID 178488260 | 91.7% |
Reaction Steps
A mixture of 13B (2.0 g, 0.0053 mol), FeCl3.6H2O (6 g) and 1,4-dioxane (20 mL) was heated to 110° C. and reacted overnight. After reaction completed, the reaction mixture was added dropwise into water. The precipitated solids were collected by filtration to give 13C (1.8 g, 90.4% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08969373B2 |
|---|
| Source dataset | uspto-grants-2015_03 |
|---|
| ORD ID | ord-404d11d24fa74ec28337283a7a32ac72 |
|---|
| Source note | uspto-grants-2015_03 |
|---|
