反应详情

温度

110 °C

A mixture of 14B (1.1 g, 2.6 mmol), MnO2 (6 g) in THF (20 mL) was heated to 110° C. and reacted overnight, then filtered. The filtrate was concentrated to give 14C (0.8 g, 73% yield).

1. customreacted overnight
2. filtrationfiltered
3. concentrationThe filtrate was concentrated