Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | HCID 86722258 | HCID 86722258 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86722259 | HCID 86722259 | 71.9% |
Reaction Steps
A mixture of 15A (2.8 g, 6.6 mmol), AcOH (10 mL) and H3PO4 (10 mL) was heated to 90° C. and reacted for 2 hours. TLC monitored the reaction. After the reaction completed, the reaction mixture was added dropwise into water. The precipitated solids were collected by filtration to give 15B (2 g, 71.4% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08969373B2 |
|---|
| Source dataset | uspto-grants-2015_03 |
|---|
| ORD ID | ord-af619ac7e3bc4702b566890ed67be1a0 |
|---|
| Source note | uspto-grants-2015_03 |
|---|
