Tetrahydrofuran → Ethyl 2,6-dichloro-3-triisopropylsilyloxybenzoate

HRID 86985Notes

Reaction equation

HRID 86985 reaction equation
[CH2:20]([Li:21])[CH2:22][CH2:23][CH3:24].[CH3:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30].[Cl:1][c:2]1[cH:3][c:4]([Cl:19])[c:5]([O:8][Si:9]([CH:10]([CH3:11])[CH3:12])([CH:13]([CH3:14])[CH3:15])[CH:16]([CH3:17])[CH3:18])[cH:6][cH:7]1.[Cl:31][C:32](=[O:33])[O:34][CH2:35][CH3:36].[O:37]1[CH2:38][CH2:39][CH2:40][CH2:41]1>>[Cl:1][c:2]1[c:3]([C:32](=[O:33])[O:34][CH2:35][CH3:36])[c:4]([Cl:19])[c:5]([O:8][Si:9]([CH:10]([CH3:11])[CH3:12])([CH:13]([CH3:14])[CH3:15])[CH:16]([CH3:17])[CH3:18])[cH:6][cH:7]1

Participants

6

Reactant 5

HCID 8028TetrahydrofuranHCID 8058HexaneHCID 10928Ethyl chloroformateHCID 19603523HCID 19603523, compoundHCID 178418339Butyllithium

Product 1

HCID 19603310Ethyl 2,6-dichloro-3-triisopropylsilyloxybenzoate

Sources & evidence

ORD record
ord-310c461feb304dd3acdbf757e0ff6483
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (2/10)

Reaction notes

Loading…