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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 870045Generated: October 30, 2026

HCID 57900985, compound → HCID 24178408, compound

https://huagongshe.com/reaction/870045

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57900985HCID 57900985—
SolventEthyl acetate hexaneHCID 21226206—
ProductHCID 24178408HCID 24178408—

Reaction Steps

Methyl 4-[(1S)-1-({[2,5-dibromo-4-(3-chlorobenzyl)-3-thienyl]carbonyl}amino)ethyl]benzoate from Example 5, Step 1 (27.0 mg, 0.0472 mmol) was reacted under conditions similar to Example 1, Step 11. After trituration of the crude product in 1:9 EtOAc/hexane, the desired product was obtained as a white solid. MS (−APCI): m/z 554 (M−1)−.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08969394B2
Source datasetuspto-grants-2015_03
ORD IDord-71576893a6bc41558b50280eb569dc78
Source noteuspto-grants-2015_03