HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57900985, compound → HCID 24178408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57900985 | HCID 57900985 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 24178408 | HCID 24178408 | — |
Reaction Steps
Methyl 4-[(1S)-1-({[2,5-dibromo-4-(3-chlorobenzyl)-3-thienyl]carbonyl}amino)ethyl]benzoate from Example 5, Step 1 (27.0 mg, 0.0472 mmol) was reacted under conditions similar to Example 1, Step 11. After trituration of the crude product in 1:9 EtOAc/hexane, the desired product was obtained as a white solid. MS (−APCI): m/z 554 (M−1)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969394B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-71576893a6bc41558b50280eb569dc78 |
| Source note | uspto-grants-2015_03 |