HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 870539Generated: October 28, 2026
Diisopropylethylamine → HCID 58072096, compound
https://huagongshe.com/reaction/870539
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 51606335 | HCID 51606335 | — |
| Reactant | HCID 58071952 | HCID 58071952 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 58072096 | HCID 58072096 | — |
Reaction Steps
100 mg 6.1 and 30 mg of (S)-4-(aminomethyl)pyrrolidin-2-one (2.2) were dissolved in dimethylacetamide. 0.175 mL of diisopropylethylamine was added and the mixture was heated at 70° C. overnight. The mixture was diluted with water and methanol and purified via chromatography (RP-HPLC) and the corresponding fractions were freeze-dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08969568B2 |
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| Source dataset | uspto-grants-2015_03 |
|---|
| ORD ID | ord-bd3c2bd0698a4aec9ec2bc3a511c7458 |
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| Source note | uspto-grants-2015_03 |
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