Trifluoroacetic acid → HCID 178525685, compound

Participants

Reaction Steps

Stir a mixture of tert-butyl 2-[2-(1H-triazol-5-yl)ethoxy]acetate (14.15 g; 62.26 mmol) and trifluoroacetic acid (70.75 mL, 935.69 mmol) in dichloromethane (70.75 mL) for 2 hours at room temperature. Concentrate the reaction mixture under reduced pressure to provide the title compound containing additional trifluoroacetic acid (20.22 g, >100%) as a brown solid. MS (m/z): 172.05 (M+1).

Provenance & Evidence