HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fluorene → HCID 22568535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fluorene | HCID 6853 | — |
| Reactant | 1-Bromooctadecane | HCID 8218 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | HCID 22568535 | HCID 22568535 | 88% |
Reaction Steps
Fluorene (7.0 g, 42.1 mmol), n-BuLi (17.35 ml, 43.4 mmol, 2.5 M in hexane), RX=1-bromooctadecane (14.53 g, 43.6 mmol). Following the usual workup 44 was isolated as a white solid (15.5 g, 88%), Rf 0.73 (cyclohexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08969624B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-5b047e7a2f364f53b7e94fa5b78fa29e |
| Source note | uspto-grants-2015_03 |