Chloroethane → HCID 70926503, compound

Participants

Reaction Steps

To a solution of 0.08 g (0.18 mmol) of the product prepared in step 10.6 in 5 mL of methanol is added 0.53 mL (0.53 mmol) of 1.0 M hydrochloric ether. The mixture is stirred for 30 minutes at room temperature and then diluted with ether. The precipitate is drained by suction, rinsed with ether and with pentane, and dried under vacuum. 0.133 g of the expected product is obtained in the form of a beige-coloured solid. Yield (dihydrochloride)=77%. m.p. >260°C. M+H+=485.

Provenance & Evidence