Hydrochloric Acid → HCID 70925882, compound

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Reaction Steps

0.11 g (0.21 mmol) of the product prepared in step 14.4 is suspended in 3 mL of anhydrous dioxane and 0.63 mL (0.63 mmol) of a 1M solution of hydrogen chloride in ether is added. The mixture is diluted with ether and the solid is then drained by suction, rinsed with pentane and dried in an oven. 0.11 g of the expected product is obtained in the form of a yellow powder. Yield (dihydrochloride)=87%. m.p.=204-206°C. M+H+=515.

Provenance & Evidence