Chloroethane → HCID 70926640, compound

Participants

Reaction Steps

To a solution of 0.25 g (0.50 mmol) of the product prepared in step 19.3 in 10 mL of a dichloromethane/methanol mixture (4/1) are added 2 mL (2 mmol) of 1.0 M hydrochloric ether. The mixture is stirred for 10 minutes at room temperature and is then diluted with ether. The precipitate is drained by suction, rinsed with ether and with pentane, and dried under vacuum. 0.28 g of the expected product is obtained in the form of a yellow solid. Yield (dihydrochloride)=96%. m.p.=200°C. (decomposition). M+H+=510.

Provenance & Evidence