Chloroethane → HCID 70926394, compound

Participants

Reaction Steps

To a suspension of 0.137 g (0.26 mmol) of the product prepared in step 21.1 in 5 mL of CH2Cl2 are added 1.05 mL (1.05 mmol) of 1.0 M hydrochloric ether. The mixture is stirred for 5 minutes at room temperature and then diluted with ether. The precipitate is drained by suction, rinsed with ether and with pentane, and dried under vacuum. 0.12 g of the expected product is obtained in the form of a yellow solid. Yield (dihydrochloride)=77%. m.p.=206°C. (decomposition). M+H+=568

Provenance & Evidence