Hydrochloric Acid → HCID 70926421, compound

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Reaction Steps

A solution of 0.065 g (0.13 mmol) of the product prepared in step 23.1 in 3 mL of CH2Cl2 is cooled on an ice bath, and 0.39 mL (0.39 mmol) of a 1M solution of hydrogen chloride in ether is added. The mixture is stirred for 10 minutes at room temperature and then poured into ether. The solid is drained by suction, rinsed with pentane and dried in an oven under vacuum. 0.059 g of the expected compound is obtained. Yield (dihydrochloride)=80%. m.p.=256°C. (decomposition). M+H+=500

Provenance & Evidence