Hydrochloric Acid → HCID 70926017, compound

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Reaction Steps

A solution of 0.07 g (0.14 mmol) of the product prepared in step 24.4 in 3 mL of methanol is cooled on an ice bath, and 0.42 mL (0.42 mmol) of a 1M solution of hydrogen chloride in ether is added. The mixture is stirred for 10 minutes at room temperature and ether is then added. The solid is drained by suction, rinsed with pentane and dried in an oven under vacuum. 0.075 g of the expected compound is obtained. Yield (dihydrochloride)=93%.

Provenance & Evidence