HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → 3-chloro-N-cyclohexylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| Product | 3-chloro-N-cyclohexylbenzamide | HCID 306824 | 70% |
Reaction Steps
Employing 0.19 g (1.9 mmol) of cyclohexylamine and 0.51 g, (2.9 mmol) of 3-chloro-benzoyl chloride in the procedure described above and elution with CHCl3/MeOH/Et3N (9.8:0.1:0.1) gave white crystals in 70% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975288B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-388c45c4d0e04b55840efcf5cbffab1e |
| Source note | uspto-grants-2015_03 |