HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentylamine → 3-chloro-N-cyclopentylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentylamine | HCID 2906 | — |
| Reactant | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| Product | 3-chloro-N-cyclopentylbenzamide | HCID 4124435 | 92% |
Reaction Steps
Employing 0.16 g (1.9 mmol) of cyclopentylamine and 0.51 g, (2.9 mmol) of 3-chloro-benzoyl chloride in the procedure described above and elution with CHCl3/MeOH/Et3N (9.8:0.1:0.1) gave white crystals in 92% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975288B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-542791f0f382422f960f4c5e087ed867 |
| Source note | uspto-grants-2015_03 |