Hydrogen Peroxide → HCID 178509298, compound

HRID 872369Notes

Reaction equation

HRID 872369 reaction equation
[OH:1][S:2]([OH:5])(=[O:4])=[O:3].[NH2:6][C:7]1[N:11]=[C:10]([SH:12])[NH:9][N:8]=1.OO>O>[S:2]([OH:5])([OH:4])(=[O:3])=[O:1].[NH2:6][C:7]1[N:11]=[C:10]([S:12][S:12][C:10]2[NH:9][N:8]=[C:7]([NH2:6])[N:11]=2)[NH:9][N:8]=1

Participants

5

Reactant 3

HCID 784Hydrogen PeroxideHCID 1118Sulfuric AcidHCID 1785092965-amino-1H-1,2,4-triazole-3-thiol

Product 1

HCID 178509298HCID 178509298, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Concentrated H2SO4 was added to a stirring mixture of 180.0 g 3-amino-1,2,4-triazole-5-thiol and 2958 g of water. A 30% hydrogen peroxide solution (87.8 g) was added and stirring was continued overnight. A peroxide test strip showed that all of the peroxide was consumed. The product is a solution of 3-amino-1,2,4-triazol-5-yl disulfide hydrogen sulfate.

Workup

  1. customwas consumed

Sources & evidence

ORD record
ord-4a9dc2e058eb4608920df5006ae9629f
Source dataset
uspto-grants-2015_03
Patent number
US08975316B2

Reaction notes

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