HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 67169035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-(3-Butynyloxy)tetrahydro-2H-pyran | HCID 142440 | — |
| Reactant | Ethyl 2-chloro-2-(hydroxyimino)acetate | HCID 6399471 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67169035 | HCID 67169035 | — |
Reaction Steps
Ethyl chlorooximidoacetate (1 g, 6.60 mmol) and 2-(but-3-ynyloxy)tetrahydro-2H-pyran (3.05 g, 19.80 mmol) were dissolved in diethyl ether (20 ml). Triethylamine (0.668 g, 6.60 mmol) was diluted with diethyl ether (10 ml) and added dropwise into previous mixture. After addition the reaction mixture was extracted with water and the organic layer was dried with Na2SO4, filtered and evaporated. LC-MS: [M+1]=172.17.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975254B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-36583926c8d44fcd9d167d7913620ef1 |
| Source note | uspto-grants-2015_03 |