HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 71243824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-(Hydroxymethyl)benzonitrile | HCID 2734677 | — |
| Reactant | HCID 86724162 | HCID 86724162 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 71243824 | HCID 71243824 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using sodium hydride (17.97 mg, 0.449 mmol) in THF (4 mL), 3-(hydroxymethyl)benzonitrile (59.8 mg, 0.449 mmol) and 7-chloro-1-isopropyl-2,3-dihydroimidazo[1,2-c]pyrimidin-5(1H)-one (80 mg, 0.374 mmol) in DMF (2.00 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-e63d4fce260d4f129500d0572f3e8fb4 |
| Source note | uspto-grants-2015_03 |