HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 71243826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 71241066 | HCID 71241066 | — |
| Reactant | 7-Chloro-1-methyl-2,3-dihydroimidazo[1,2-C]pyrimidin-5(1H)-one | HCID 71743458 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 71243826 | HCID 71243826 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using NaH (17.46 mg, 0.727 mmol), (3-fluoro-4-(5-methyl-1H-imidazol-1-yl)phenyl)methanol (100 mg, 0.485 mmol) in THF (8 mL) and 7-chloro-1-methyl-2,3-dihydroimidazo[1,2-c]-pyrimidin-5(1H)-one (90 mg, 0.485 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-8cec221f62b1435b97ab2a2640f303b2 |
| Source note | uspto-grants-2015_03 |