HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 71243754, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | (4-(4-Chloro-3-(trifluoromethyl)phenoxy)phenyl)methanol | HCID 66825563 | — |
| Reactant | HCID 86724162 | HCID 86724162 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 71243754 | HCID 71243754 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using (4-(4-chloro-3-(trifluoromethyl)phenoxy)phenyl)methanol (50 mg, 0.165 mmol), NaH (11.89 mg, 0.496 mmol) in 5 mL and 7-chloro-1-isopropyl-2,3-dihydroimidazo[1,2-c]pyr-imidin-5(1H)-one (52.9 mg, 0.248 mmol) in DMF (5 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-cf9c33b872a442e1b2cfc3883023d5dd |
| Source note | uspto-grants-2015_03 |