HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 71243724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 66825535 | HCID 66825535 | — |
| Reactant | Tert-butyl 7-chloro-5-oxo-2,3-dihydroimidazo[1,2-C]pyrimidine-1(5H)-carboxylate | HCID 71743561 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 71243724 | HCID 71243724 | — |
Reaction Steps
Prepared in a manner similar to that described for E65 using sodium hydride (13.87 mg, 0.347 mmol), (3-chloro-4-(3-(trifluoromethyl)phenoxy)phenyl)methanol in THF (8 mL) and tert-butyl 7-chloro-5-oxo-2,3-dihydroimidazo[1,2-c]pyrimidine-1(5H)-carboxylate (62.8 mg, 0.231 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-d7c43dbabce94ab08a63f6209d3f71d2 |
| Source note | uspto-grants-2015_03 |